N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfinylacetamide

Base Information

Chemical Name:N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfinylacetamide
CAS No.:374593-79-0
Molecular Formula:C₂₃H₂₁NO₅S
Molecular Weight:423.489
Hs Code.:

Synonyms:N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfinylacetamide

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Chemical Property of N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfinylacetamide

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Technology Process of N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfinylacetamide

There total 6 articles about N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfinylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 374593-76-7
N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfanylacetamide

: 374593-79-0
N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfinylacetamide

Guidance literature:: With sodium periodate; In methanol; water; for 2h; Heating;
DOI:10.1248/cpb.49.1132

Reference yield:

: 7031-27-8
(phenylthio)acetic acid chloride

: 374593-79-0
N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfinylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 22.6 g / Et₃N / benzene / 20 h / 20 °C

2: 99 percent / NaIO₄ / methanol; H₂O / 2 h / Heating

With sodium periodate; triethylamine; In methanol; water; benzene;
DOI:10.1248/cpb.49.1132

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 374593-79-0
N-(3-methoxyphenyl)-N-(3,4-methylenedioxyphenyl)methyl-2-phenylsulfinylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: Ti(i-PrO)4 / 3 h / 80 °C

1.2: 99 percent / NaBH₄ / methanol / 1 h / 20 °C

2.1: 22.6 g / Et₃N / benzene / 20 h / 20 °C

3.1: 99 percent / NaIO₄ / methanol; H₂O / 2 h / Heating

With titanium(IV) isopropylate; sodium periodate; triethylamine; In methanol; water; benzene;
DOI:10.1248/cpb.49.1132