trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2]thiocyanate

Base Information

Chemical Name:trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2]thiocyanate
CAS No.:441772-29-8
Molecular Formula:CNS*C₃₂H₃₀CoN₆O₂
Molecular Weight:647.706
Hs Code.:

Synonyms:trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2]thiocyanate

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Chemical Property of trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2]thiocyanate

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Technology Process of trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2]thiocyanate

There total 1 articles about trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2]thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 70559-56-7
[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)]hydrate

: 333-20-0
potassium thioacyanate

: 100-46-9
benzylamine

: 441772-29-8
trans-[Co(N,N'-bis(2-pyridinecarboxamide)-1,2-benzene dianion)(benzylamine)2]thiocyanate

Guidance literature:: With air; In methanol; to soln. of Co-complex in MeOH added dropwise benzylamine; air bubbled for 3 h, MeOH added during this period; mixt. filtered off; soln. of KCNSin MeOH added to filtrate; EtOH added; after 48 h crystals filtered; washed (EtOH-ether); dried (vac.); elem. anal.;
DOI:10.1016/S0020-1693(02)00906-4