C₂₂H₂₂N₂

Base Information

• Chemical Name: C₂₂H₂₂N₂
• CAS No.: 853119-19-4
• Molecular Formula: C₂₂H₂₂N₂
• Molecular Weight: 314.43
• Mol file: 853119-19-4.mol

Synonyms:C₂₂H₂₂N₂

Chemical Property of C₂₂H₂₂N₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₂N₂

There total 3 articles about C₂₂H₂₂N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

N-ethyl-3-carbazolealdehyde (7570-45-8) + benzylamine (100-46-9) → C22H22N2 (853119-19-4)

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; at 20 ℃; for 18h;

DOI:10.1071/CH16169

Reference yield:

9H-carbazole (86-74-8,105184-46-1,97960-57-1) → C22H22N2 (853119-19-4)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide / 18 h / 20 °C

2: titanium tetrachloride / dichloromethane / 4 h / -78 °C

3: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / 18 h / 20 °C

With titanium tetrachloride; sodium tris(acetoxy)borohydride; sodium hydride; acetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2: |Rieche Formylation;

DOI:10.1071/CH16169

Reference yield:

N-ethylcarbazole (86-28-2) → C22H22N2 (853119-19-4)

Guidance literature:

Multi-step reaction with 2 steps

1: titanium tetrachloride / dichloromethane / 4 h / -78 °C

2: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / 18 h / 20 °C

With titanium tetrachloride; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; dichloromethane; 1: |Rieche Formylation;

DOI:10.1071/CH16169

upstream raw materials:

N-ethyl-3-carbazolealdehyde

benzylamine

9H-carbazole

N-ethylcarbazole