N-<2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide

Base Information

Chemical Name:N-<2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide
CAS No.:155344-87-9
Molecular Formula:C₂₄H₃₁NO₅Si
Molecular Weight:441.599
Hs Code.:

Synonyms:N-<2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide

Suppliers and Price of N-<2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide

Chemical Property:

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Technology Process of N-<2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide

There total 5 articles about N-<2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 155344-84-6
N-<2-(hydroxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide

: 155344-87-9
N-<2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 25 ℃; for 24h;
DOI:10.1016/S0040-4020(01)87039-3

Reference yield:

: 85-44-9
phthalic anhydride

: 155344-87-9
N-<2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / 1.5 h / 150 °C

2: NBS / CCl₄ / Heating; Irradiation

3: H₂O / tetrahydrofuran / Ambient temperature

4: 93 percent / imidazole / dimethylformamide / 24 h / 25 °C

With 1H-imidazole; N-Bromosuccinimide; water; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)87039-3

Reference yield:

: 26477-09-8
N-2-(3,4-dimethoxyphenyl)ethylphthalimide

: 155344-87-9
N-<2-(t-butyldimethylsilyloxy)-2-(3,4-dimethoxyphenyl)ethyl>phthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: NBS / CCl₄ / Heating; Irradiation

2: H₂O / tetrahydrofuran / Ambient temperature

3: 93 percent / imidazole / dimethylformamide / 24 h / 25 °C

With 1H-imidazole; N-Bromosuccinimide; water; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)87039-3