(E)-6-(N-(3-phenylprop-2-ynyl)-N-tosylamino)hex-4-en-1-yn-3-yl pivalate

Base Information

Chemical Name:(E)-6-(N-(3-phenylprop-2-ynyl)-N-tosylamino)hex-4-en-1-yn-3-yl pivalate
CAS No.:1334209-47-0
Molecular Formula:C₂₇H₂₉NO₄S
Molecular Weight:463.598
Hs Code.:

Synonyms:(E)-6-(N-(3-phenylprop-2-ynyl)-N-tosylamino)hex-4-en-1-yn-3-yl pivalate

Suppliers and Price of (E)-6-(N-(3-phenylprop-2-ynyl)-N-tosylamino)hex-4-en-1-yn-3-yl pivalate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-6-(N-(3-phenylprop-2-ynyl)-N-tosylamino)hex-4-en-1-yn-3-yl pivalate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-6-(N-(3-phenylprop-2-ynyl)-N-tosylamino)hex-4-en-1-yn-3-yl pivalate

There total 9 articles about (E)-6-(N-(3-phenylprop-2-ynyl)-N-tosylamino)hex-4-en-1-yn-3-yl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₁NO₃S

: 3282-30-2
pivaloyl chloride

: 1334209-47-0
(E)-6-(N-(3-phenylprop-2-ynyl)-N-tosylamino)hex-4-en-1-yn-3-yl pivalate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201103136

Reference yield:

: 944045-59-4
C₂₀H₂₁NO₃S

: 1334209-47-0
(E)-6-(N-(3-phenylprop-2-ynyl)-N-tosylamino)hex-4-en-1-yn-3-yl pivalate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium chlorochromate / dichloromethane / 0 - 20 °C / Inert atmosphere; Molecular sieve

2: tetrahydrofuran / 20 °C / Inert atmosphere

3: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere

With dmap; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201103136

Reference yield:

: C₂₂H₂₃NO₄S

: 1334209-47-0
(E)-6-(N-(3-phenylprop-2-ynyl)-N-tosylamino)hex-4-en-1-yn-3-yl pivalate

Guidance literature:: Multi-step reaction with 4 steps

1: methanol; potassium carbonate / 6 h / 20 °C / Inert atmosphere

2: pyridinium chlorochromate / dichloromethane / 0 - 20 °C / Inert atmosphere; Molecular sieve

3: tetrahydrofuran / 20 °C / Inert atmosphere

4: dmap; triethylamine / dichloromethane / 20 °C / Inert atmosphere

With methanol; dmap; potassium carbonate; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201103136