N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

Base Information

Chemical Name:N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide
CAS No.:1127943-68-3
Molecular Formula:C₁₈H₂₃BrN₂O₅SSi
Molecular Weight:487.447
Hs Code.:

Synonyms:N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

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Technology Process of N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

There total 2 articles about N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1127943-39-8
2-{3-bromo-5-(trimethylsilyl)-4-[(trimethylsilyl)oxy]phenyl}ethyl methanesulfonate

: 6319-45-5
N-methyl-4-nitro-benzenesulfonamide

: 1127943-68-3
N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

Guidance literature:: N-methyl-4-nitro-benzenesulfonamide; With sodium hydride; In N,N-dimethyl-formamide; for 0.5h;

2-{3-bromo-5-(trimethylsilyl)-4-[(trimethylsilyl)oxy]phenyl}ethyl methanesulfonate; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jo802728u

Reference yield: 88.0%

: 1127943-34-3
(3-bromo-2-[(trimethylsilyl)oxy]-5-{2-[(trimethylsilyl)oxy]ethyl}phenyl)(trimethyl)silane

: 6319-45-5
N-methyl-4-nitro-benzenesulfonamide

: 1127943-68-3
N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2010.03.096

Reference yield: 44.0%

: 529-28-2
4-iodoanisol

: 1127943-68-3
N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

: 1127943-83-2
C₂₅H₂₈BrIN₂O₆SSi

Guidance literature:: With [bis(acetoxy)iodo]benzene; In 1,1,1,3',3',3'-hexafluoro-propanol; at 0 ℃; for 0.0388889h; regioselective reaction;
DOI:10.1021/jo802728u