N-{2-[3-bromo-1-(4-methoxyphenyl)-4-oxo-5-(trimethylsilyl)-cyclohexa-2,5-dien-1-yl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

Base Information

• Chemical Name: N-{2-[3-bromo-1-(4-methoxyphenyl)-4-oxo-5-(trimethylsilyl)-cyclohexa-2,5-dien-1-yl]ethyl}-N-methyl-4-nitrobenzenesulfonamide
• CAS No.: 1127943-41-2
• Molecular Formula: C₂₅H₂₉BrN₂O₆SSi
• Molecular Weight: 593.571

Synonyms:N-{2-[3-bromo-1-(4-methoxyphenyl)-4-oxo-5-(trimethylsilyl)-cyclohexa-2,5-dien-1-yl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

Chemical Property of N-{2-[3-bromo-1-(4-methoxyphenyl)-4-oxo-5-(trimethylsilyl)-cyclohexa-2,5-dien-1-yl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

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Technology Process of N-{2-[3-bromo-1-(4-methoxyphenyl)-4-oxo-5-(trimethylsilyl)-cyclohexa-2,5-dien-1-yl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

There total 1 articles about N-{2-[3-bromo-1-(4-methoxyphenyl)-4-oxo-5-(trimethylsilyl)-cyclohexa-2,5-dien-1-yl]ethyl}-N-methyl-4-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide (1127943-68-3) + methoxybenzene (100-66-3) → N-{2-[3-bromo-1-(4-methoxyphenyl)-4-oxo-5-(trimethylsilyl)-cyclohexa-2,5-dien-1-yl]ethyl}-N-methyl-4-nitrobenzenesulfonamide (1127943-41-2)

Guidance literature:

With [bis(acetoxy)iodo]benzene; In 1,1,1,3',3',3'-hexafluoro-propanol; at 0 ℃; for 0.0388889h; regioselective reaction;

DOI:10.1021/jo802728u

Reference yield: 71.0%

N-{2-[3-bromo-1-(4-methoxyphenyl)-4-oxo-5-(trimethylsilyl)-cyclohexa-2,5-dien-1-yl]ethyl}-N-methyl-4-nitrobenzenesulfonamide (1127943-41-2) + thiophenol (108-98-5) → 3a-(4-methoxyphenyl)-1-methyl-5-(phenylthio)-1,2,3,3a,7,7a-hexahydro-6H-indol-6-one

Guidance literature:

With potassium carbonate; In acetonitrile;

DOI:10.1021/jo802728u

Reference yield: 71.0%

N-{2-[3-bromo-1-(4-methoxyphenyl)-4-oxo-5-(trimethylsilyl)-cyclohexa-2,5-dien-1-yl]ethyl}-N-methyl-4-nitrobenzenesulfonamide (1127943-41-2) + thiophenol (108-98-5) → C22H23NO2S

Guidance literature:

With potassium carbonate; In acetonitrile;

DOI:10.1016/j.tet.2010.03.096

upstream raw materials:

N-{2-[3-bromo-4-hydroxy-5-(trimethylsilyl)phenyl]ethyl}-N-methyl-4-nitrobenzenesulfonamide

methoxybenzene

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