phenylmethyl formyl{(2E)-4-[(triphenylmethyl)oxy]but-2-en-1-yl}carbamate

Base Information

• Chemical Name: phenylmethyl formyl{(2E)-4-[(triphenylmethyl)oxy]but-2-en-1-yl}carbamate
• CAS No.: 1315127-88-8
• Molecular Formula: C₃₂H₂₉NO₄
• Molecular Weight: 491.587

Synonyms:phenylmethyl formyl{(2E)-4-[(triphenylmethyl)oxy]but-2-en-1-yl}carbamate

Chemical Property of phenylmethyl formyl{(2E)-4-[(triphenylmethyl)oxy]but-2-en-1-yl}carbamate

Chemical Property:

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Technology Process of phenylmethyl formyl{(2E)-4-[(triphenylmethyl)oxy]but-2-en-1-yl}carbamate

There total 2 articles about phenylmethyl formyl{(2E)-4-[(triphenylmethyl)oxy]but-2-en-1-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

cinnamyl methyl carbonate + benzyl formylcarbamate (69261-49-0) → (+)-phenylmethyl formyl((1S)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate (1315127-86-6) + phenylmethyl formyl{(2E)-4-[(triphenylmethyl)oxy]but-2-en-1-yl}carbamate (1315127-88-8)

Guidance literature:

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₃₂NO₃P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; In tetrahydrofuran; at 20 ℃; for 1h; enantioselective reaction; Inert atmosphere;

DOI:10.1002/chem.201100649

Reference yield:

cinnamyl methyl carbonate + benzyl formylcarbamate (69261-49-0) → phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate (1315128-16-5) + phenylmethyl formyl{(2E)-4-[(triphenylmethyl)oxy]but-2-en-1-yl}carbamate (1315127-88-8)

Guidance literature:

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₃₂NO₃P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; In tetrahydrofuran; at 20 ℃; for 1h; enantioselective reaction; Inert atmosphere;

DOI:10.1002/chem.201100649

upstream raw materials:

benzyl formylcarbamate

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