phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

Base Information

Chemical Name:phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate
CAS No.:1315128-16-5
Molecular Formula:C₃₂H₂₉NO₄
Molecular Weight:491.587
Hs Code.:

Synonyms:phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

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Chemical Property of phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

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Technology Process of phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

There total 1 articles about phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cinnamyl methyl carbonate

: 69261-49-0
benzyl formylcarbamate

: 1315128-16-5
phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

: 1315127-88-8
phenylmethyl formyl{(2E)-4-[(triphenylmethyl)oxy]but-2-en-1-yl}carbamate

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₃₂NO₃P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; In tetrahydrofuran; at 20 ℃; for 1h; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.201100649

Reference yield: 88.0%

: 1315128-16-5
phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

: 174626-07-4
(+)-phenylmethyl ((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 1h;
DOI:10.1002/chem.201100649

Reference yield:

: 1315128-16-5
phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

: C₃₉H₄₄BNO₃

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / methanol / 1 h / 20 °C

2: tetrahydrofuran / 3 h / 50 °C / Inert atmosphere

With potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1002/chem.201100649