[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germanethione

Base Information

Chemical Name:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germanethione
CAS No.:152291-63-9
Molecular Formula:C₄₂H₈₂GeSSi₆
Molecular Weight:860.282
Hs Code.:

Synonyms:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germanethione

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Chemical Property of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germanethione

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Technology Process of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germanethione

There total 7 articles about [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germanethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.7%

: 152291-64-0
5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane

: 152291-63-9
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germanethione

Guidance literature:: With triphenyl phosphine; In hexane; byproducts: Ph3PS; refluxed for 2 h; under argon, filtrated and concd.;

Reference yield: 96.0%

: 152291-64-0
5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane

: 603-35-0
triphenylphosphine

: 152291-63-9
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germanethione

: 3878-45-3
triphenylphosphine sulfide

Guidance literature:: In hexane; refluxing (2 h),; filtration, concentration (Ar);
DOI:10.1021/ja991147x

Reference yield:

: 162088-75-7
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

: 152291-63-9
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germanethione

Guidance literature:: Multi-step reaction with 3 steps

1: LiC₁₀H₈ / tetrahydrofuran

3: hexane

With LiC₁₀H₈; In tetrahydrofuran; hexane;
DOI:10.1021/ja991147x