5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane

Base Information

Chemical Name:5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane
CAS No.:152291-64-0
Molecular Formula:C₄₂H₈₂GeS₄Si₆
Molecular Weight:956.48
Hs Code.:

Synonyms:5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane

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Chemical Property of 5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane

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Technology Process of 5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane

There total 7 articles about 5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 10544-50-0
sulfur

: 162088-71-3
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)bromochloro(2,4,6-triisopropylphenyl)germane

: 152291-64-0
5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane

Guidance literature:: With t-BuLi; In 1,2-dimethoxyethane; pentane; Ar-atmosphere; stirring (-78°C, 5 min), S8 addn., refluxing (10 h); evapn. (reduced pressure), recrystn. (CHCl3), chromy. (SiO2, hexane), recrystn. (EtOH); elem. anal.;
DOI:10.1021/om00002a055

Reference yield: 68.0%

: 10544-50-0
sulfur

: 152291-69-5
{2,4,6-tris(bis(trimethylsilyl)methyl)phenyl}(2,4,6-triisopropylphenyl)germylene

: 152291-64-0
5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane

Guidance literature:: stiring (5 h); chromatography (SiO2, CH2Cl2), GPLC, pptn. (CH2Cl2/hexane);
DOI:10.1021/ja991147x

Reference yield: 65.0%

: 10544-50-0
sulfur

: 162088-73-5
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane

: 152291-64-0
5-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-5-(2,4,6-triisopropylphenyl)-1,2,3,4,5-tetrathiagermolane

Guidance literature:: Ar-atmosphere; 160°C (30 min); recrystn. (CHCl3), chromy. (SiO2, hexane), recrystn. (EtOH); elem. anal.;
DOI:10.1021/om00002a055