(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

Base Information

Chemical Name:(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane
CAS No.:162088-75-7
Molecular Formula:C₄₂H₈₂Br₂GeSi₆
Molecular Weight:988.024
Hs Code.:

Synonyms:(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

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Chemical Property of (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

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Technology Process of (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

There total 2 articles about (2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 128-08-5
N-Bromosuccinimide

: 162088-73-5
[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl](2,4,6-triisopropylphenyl)germane

: 162088-75-7
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

Guidance literature:: In benzene; Ar-atmosphere; stirring (room temp., 10 h); chromy. (SiO2, C6H6), repptn. (CHCl3 / EtOH, room temp.); elem. anal.;
DOI:10.1021/om00002a055

Reference yield:

: 115160-05-9
1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene

: 162088-75-7
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

Guidance literature:: Multi-step reaction with 3 steps

1: t-BuLi; NH₄Cl / tetrahydrofuran; pentane

2: NH₄Cl / tetrahydrofuran; water

3: benzene

With t-BuLi; NH₄Cl; In tetrahydrofuran; water; pentane; benzene;
DOI:10.1021/om00002a055

Reference yield: 87.0%

: 162088-75-7
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)dibromo(2,4,6-triisopropylphenyl)germane

: 2904-57-6
mesitylenecarbonitrile oxide

: 163773-48-6
[(CH₃)2CH]3C₆H₂GeCNO[C₆H₂(CH₃)3]C₆H₂[CH(Si(CH₃)3)2]3

Guidance literature:: With lithium naphthalenide; In tetrahydrofuran; react. of ge-compound with LiC10H7, react. with nirile oxide;
DOI:10.1039/a703241b