bis(1,2-bis(diethylphosphino)ethane)(η2-dihydrogen)hydridoosmium(II) tetraphenylborate

Base Information

Chemical Name:bis(1,2-bis(diethylphosphino)ethane)(η2-dihydrogen)hydridoosmium(II) tetraphenylborate
CAS No.:108150-71-6
Molecular Formula:C₂₀H₅₁OsP₄*C₂₄H₂₀B
Molecular Weight:924.954
Hs Code.:

Synonyms:bis(1,2-bis(diethylphosphino)ethane)(η2-dihydrogen)hydridoosmium(II) tetraphenylborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(1,2-bis(diethylphosphino)ethane)(η2-dihydrogen)hydridoosmium(II) tetraphenylborate

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Technology Process of bis(1,2-bis(diethylphosphino)ethane)(η2-dihydrogen)hydridoosmium(II) tetraphenylborate

There total 3 articles about bis(1,2-bis(diethylphosphino)ethane)(η2-dihydrogen)hydridoosmium(II) tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 32914-91-3
trans-[OsH(Cl)(PEt₂(CH₂)2PEt₂)2]

: 143-66-8
sodium tetraphenyl borate

: 108150-71-6
bis(1,2-bis(diethylphosphino)ethane)(η2-dihydrogen)hydridoosmium(II) tetraphenylborate

Guidance literature:: With hydrogen; In acetone; byproducts: NaCl; to a soln. of the Os-compd. in acetone NaBPh4 is added under Ar, stirring for 30 min under H2; filtn., concn. of the filtrate and addn. of MeOH causes precipitation of the white product, elem. anal.;

Reference yield:

: 32914-91-3
trans-[OsH(Cl)(PEt₂(CH₂)2PEt₂)2]

: 143-66-8
sodium tetraphenyl borate

: deuterium hydride

: 108150-71-6
bis(1,2-bis(diethylphosphino)ethane)(η2-dihydrogen)hydridoosmium(II) tetraphenylborate

: trans-{Os(D)(depe)2(η2-H2)}BPh4

: trans-{Os(H)(depe)2(η2-HD)}BPh4

Guidance literature:: In acetone; byproducts: NaCl; to a soln. of the Os-compd. in acetone NaBPh4 is added under Ar, stirring for 30 min under HD; filtn., concn. of the filtrate and addn. of MeOH causes precipitation of the product;