2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetic acid

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Chemical Name:2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetic acid
CAS No.:1207314-61-1
Molecular Formula:C₂₈H₂₂F₈N₂O₄
Molecular Weight:602.481
Hs Code.:

Synonyms:2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetic acid

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Chemical Property of 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetic acid

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Technology Process of 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetic acid

There total 8 articles about 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1207314-60-0
methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate

: 1207314-61-1
2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetic acid

Guidance literature:: methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate; With water; sodium hydroxide; In methanol; for 2h;

With hydrogenchloride; In water; pH=1;

Reference yield:

: 3970-35-2
2-chloro-3-nitrobezoic acid

: 1207314-61-1
2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetic acid

Guidance literature:: Multi-step reaction with 8 steps

1.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 2 h / 80 °C

2.1: pyridine / tetrahydrofuran / 5 h / 20 °C

3.1: potassium fluoride / N,N-dimethyl-formamide / 3 h / 150 °C / Molecular sieve

4.1: hydrogenchloride; tin(ll) chloride / ethanol / 1.5 h / 60 °C

4.2: 20 °C

5.1: sulfuric acid / water / 4 h / 30 - 40 °C

6.1: pyridine / tetrahydrofuran / 3 h / 20 °C

7.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

7.2: 3 h / 60 °C

8.1: water; sodium hydroxide / methanol / 2 h

8.2: pH 1

With pyridine; hydrogenchloride; potassium fluoride; thionyl chloride; sulfuric acid; water; sodium hydride; tin(ll) chloride; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 847622-62-2
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-nitrobenzamide

: 1207314-61-1
2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; tin(ll) chloride / ethanol / 1.5 h / 60 °C

1.2: 20 °C

2.1: sulfuric acid / water / 4 h / 30 - 40 °C

3.1: pyridine / tetrahydrofuran / 3 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

4.2: 3 h / 60 °C

5.1: water; sodium hydroxide / methanol / 2 h

5.2: pH 1

With pyridine; hydrogenchloride; sulfuric acid; water; sodium hydride; tin(ll) chloride; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;