methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate

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Chemical Name:methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate
CAS No.:1207314-60-0
Molecular Formula:C₂₉H₂₄F₈N₂O₄
Molecular Weight:616.508
Hs Code.:

Synonyms:methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate

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Chemical Property of methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate

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Technology Process of methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate

There total 7 articles about methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 862134-13-2
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide

: 96-32-2
bromoacetic acid methyl ester

: 1207314-60-0
methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate

Guidance literature:: N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

bromoacetic acid methyl ester; In N,N-dimethyl-formamide; at 60 ℃; for 3h;

Reference yield:

: 3970-35-2
2-chloro-3-nitrobezoic acid

: 1207314-60-0
methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 2 h / 80 °C

2.1: pyridine / tetrahydrofuran / 5 h / 20 °C

3.1: potassium fluoride / N,N-dimethyl-formamide / 3 h / 150 °C / Molecular sieve

4.1: hydrogenchloride; tin(ll) chloride / ethanol / 1.5 h / 60 °C

4.2: 20 °C

5.1: sulfuric acid / water / 4 h / 30 - 40 °C

6.1: pyridine / tetrahydrofuran / 3 h / 20 °C

7.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

7.2: 3 h / 60 °C

With pyridine; hydrogenchloride; potassium fluoride; thionyl chloride; sulfuric acid; sodium hydride; tin(ll) chloride; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 847622-62-2
N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-nitrobenzamide

: 1207314-60-0
methyl 2-(N-(2,6-dimethyl-4-(perfluoropropan-2-yl)phenyl)-2-fluoro-3-(N-methylbenzamide)benzamide)acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; tin(ll) chloride / ethanol / 1.5 h / 60 °C

1.2: 20 °C

2.1: sulfuric acid / water / 4 h / 30 - 40 °C

3.1: pyridine / tetrahydrofuran / 3 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

4.2: 3 h / 60 °C

With pyridine; hydrogenchloride; sulfuric acid; sodium hydride; tin(ll) chloride; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;