2,9-bis[p-(formyl)phenyl]-1,10-phenanthroline

Base Information

• Chemical Name: 2,9-bis[p-(formyl)phenyl]-1,10-phenanthroline
• CAS No.: 120085-99-6
• Molecular Formula: C₂₆H₁₆N₂O₂
• Molecular Weight: 388.425
• Mol file: 120085-99-6.mol

Synonyms:2,9‐bis(4-formylphenyl)‐1,10‐phenanthroline

Chemical Property of 2,9-bis[p-(formyl)phenyl]-1,10-phenanthroline

Chemical Property:

• Boiling Point: 657.3±55.0 °C(Predicted)
• PKA: 3.86±0.30(Predicted)
• Density: 1.303±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

4,4-(1,10-Phenanthroline-2,9-diyl)bis[benzaldehyde] 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,9-bis[p-(formyl)phenyl]-1,10-phenanthroline

There total 15 articles about 2,9-bis[p-(formyl)phenyl]-1,10-phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,9-bis[p-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl]-1,10-phenanthroline (321697-17-0) → 2,9‐bis(4-formylphenyl)‐1,10‐phenanthroline (120085-99-6)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; at 50 ℃; for 15h;

DOI:10.1021/ja002018f

Reference yield: 95.0%

4-formylphenylboronic acid, (87199-17-5) + 2,9-dibromo-1,10-phenanthroline (39069-02-8) → 2,9‐bis(4-formylphenyl)‐1,10‐phenanthroline (120085-99-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; water; at 100 ℃; for 13h; Schlenk technique; Inert atmosphere;

DOI:10.1021/jacs.1c02789

Reference yield: 87.0%

2,9-bis(p-hydroxymethylphenyl)-1,10-phenanthroline (157523-11-0) → 2,9‐bis(4-formylphenyl)‐1,10‐phenanthroline (120085-99-6)

Guidance literature:

With manganese(IV) oxide; In acetone; for 1h; Ambient temperature;

DOI:10.1039/DT9940001649

upstream raw materials:

2,9-bis(4-(dibromomethyl)phenyl)-1,10-phenanthroline

2,9-bis-(4-methylphenyl)-1,10-phenanthroline

propionic acid

2,9-bis(p-hydroxymethylphenyl)-1,10-phenanthroline

Downstream raw materials:

5,10,15,20-tetrakis-(3,5-di-tert-butylphenyl)porphyrin

C₁₄₈H₁₆₀N₁₀

[[(CHC₅H₂N(C₆H₄(OC₂H₄)2OCH₂))2]Cu(2,9-bis-(p-formylphenyl)-1,10-phenanthroline)](PF₆)

AuC₂₀H₈N₄(C₆H₃(C(CH₃)3)2)3C₆H₃(C₆H₄(CH₂)4O₃)2(C₁₂H₆N₂)(C₁₂H₆N₂(C₆H₄CHO)2)Cu⁽²⁺⁾

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 120085-99-6 2,9-bis[p-(formyl)phenyl]-1,10-phenanthroline

Send

Send

Metric Ton KG G Pound L ML

Send

Send