ethyl 3-[2-(4-cyanobenzyloxy)-4-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-7-carbonylamino]proanoate

Base Information

Chemical Name:ethyl 3-[2-(4-cyanobenzyloxy)-4-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-7-carbonylamino]proanoate
CAS No.:1056736-79-8
Molecular Formula:C₂₃H₂₃N₃O₆
Molecular Weight:437.452
Hs Code.:

Synonyms:ethyl 3-[2-(4-cyanobenzyloxy)-4-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-7-carbonylamino]proanoate

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Chemical Property of ethyl 3-[2-(4-cyanobenzyloxy)-4-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-7-carbonylamino]proanoate

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Technology Process of ethyl 3-[2-(4-cyanobenzyloxy)-4-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-7-carbonylamino]proanoate

There total 1 articles about ethyl 3-[2-(4-cyanobenzyloxy)-4-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-7-carbonylamino]proanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.2%

: 852233-84-2
2-[(4-cyanobenzyl)oxy]-4-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-7-carboxylic acid

: 924-73-2
3-amino-propionic acid ethyl ester

: 1056736-79-8
ethyl 3-[2-(4-cyanobenzyloxy)-4-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-7-carbonylamino]proanoate

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1,2-dichloro-ethane; In N,N-dimethyl-formamide; at 20 ℃; pH=7;
DOI:10.1021/jm8003448

Reference yield:

: 1056736-79-8
ethyl 3-[2-(4-cyanobenzyloxy)-4-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-7-carbonylamino]proanoate

: C₂₃H₂₆N₄O₆

Guidance literature:: ethyl 3-[2-(4-cyanobenzyloxy)-4-methyl-3-oxo-3,4-dihydro-2H-1,4-benzoxazine-7-carbonylamino]proanoate; With hydrogenchloride; In dichloromethane; at 20 ℃; for 48h;

With ammonium acetate; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1021/jm8003448