bis(triphenylstannyl)tellurium

Base Information

Chemical Name:bis(triphenylstannyl)tellurium
CAS No.:4324-29-2
Molecular Formula:C₃₆H₃₀Sn₂Te
Molecular Weight:827.654
Hs Code.:

Synonyms:bis(triphenylstannyl)tellurium

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Chemical Property of bis(triphenylstannyl)tellurium

Chemical Property:

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Technology Process of bis(triphenylstannyl)tellurium

There total 2 articles about bis(triphenylstannyl)tellurium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 14683-12-6
tellurium

: 1064-10-4
hexaphenylditin

: 4324-29-2
bis(triphenylstannyl)tellurium

Guidance literature:: With catalyst: tri-tert-butyl phosphine; In benzene; distannane, Te and phosphine placed in Schlenk tube under N2 atm. and dry benzene added, stirred at 80°C for 5 h; filtered under N2 to remove excess of Te, solvent evapd. in vac., residue washed with pentane, recrystd. in CH2Cl2-pentane, elem. anal.;
DOI:10.1021/om990728s

Reference yield: 93.5%

: 12034-41-2
disodium telluride

: 639-58-7
triphenyltin chloride

: 4324-29-2
bis(triphenylstannyl)tellurium

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; Ar atmosphere, addn. of soln. of Sn compound to a boiling suspension of Na2Te with stirring, stirring (reflux, 2 h); pptn. of NaCl (benzene), filtration, evapn. to dryness (vacuum), drying (70°C, 24 h); elem. anal.;

Reference yield:

: 421-17-0
Trifluoromethylsulfenyl chloride

: 4324-29-2
bis(triphenylstannyl)tellurium

: 639-58-7
triphenyltin chloride

Guidance literature:: In further solvent(s); byproducts: Te(SCF3)2; Ar atmosphere, condensation of 2-methylbutane and CF3SCl at -196°C into an evacuated Carius tube with stirring and exclusion of light, warming to 20°C, stirring (4 h); fractional condensation of organic product Te(SCF3)2 int a trap at -50°C, not isolated;