ethyl 6-O-benzyl-3-O-levulinoyl-2-deoxy-2-N-trichloroacetamidothio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 6-O-benzyl-3-O-levulinoyl-2-deoxy-2-N-trichloroacetamidothio-β-D-glucopyranoside
CAS No.:1557228-38-2
Molecular Formula:C₂₂H₂₈Cl₃NO₇S
Molecular Weight:556.892
Hs Code.:

Synonyms:ethyl 6-O-benzyl-3-O-levulinoyl-2-deoxy-2-N-trichloroacetamidothio-β-D-glucopyranoside

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Chemical Property of ethyl 6-O-benzyl-3-O-levulinoyl-2-deoxy-2-N-trichloroacetamidothio-β-D-glucopyranoside

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Technology Process of ethyl 6-O-benzyl-3-O-levulinoyl-2-deoxy-2-N-trichloroacetamidothio-β-D-glucopyranoside

There total 7 articles about ethyl 6-O-benzyl-3-O-levulinoyl-2-deoxy-2-N-trichloroacetamidothio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1557228-37-1
C₂₂H₂₆Cl₃NO₇S

: 1557228-38-2
ethyl 6-O-benzyl-3-O-levulinoyl-2-deoxy-2-N-trichloroacetamidothio-β-D-glucopyranoside

Guidance literature:: C₂₂H₂₆Cl₃NO₇S; With triethylsilane; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; Molecular sieve;
DOI:10.1039/c3cc48860h

Reference yield:

: 399035-88-2
ethyl 4,6-O-benzylidene-2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside

: 1557228-38-2
ethyl 6-O-benzyl-3-O-levulinoyl-2-deoxy-2-N-trichloroacetamidothio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 18 h / 20 °C

2.1: triethylsilane / dichloromethane / 0.5 h / 20 °C / Molecular sieve

2.2: 0 - 20 °C / Molecular sieve

With pyridine; triethylsilane; In dichloromethane;
DOI:10.1039/c3cc48860h

Reference yield:

: 635684-80-9
ethyl 2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside

: 1557228-38-2
ethyl 6-O-benzyl-3-O-levulinoyl-2-deoxy-2-N-trichloroacetamidothio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: camphor-10-sulfonic acid / N,N-dimethyl-formamide / 4 h / 65 °C

2.1: pyridine / dichloromethane / 18 h / 20 °C

3.1: triethylsilane / dichloromethane / 0.5 h / 20 °C / Molecular sieve

3.2: 0 - 20 °C / Molecular sieve

With pyridine; triethylsilane; camphor-10-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3cc48860h