ethyl 4,6-O-benzylidene-2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 4,6-O-benzylidene-2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside
CAS No.:399035-88-2
Molecular Formula:C₁₇H₂₀Cl₃NO₅S
Molecular Weight:456.774
Hs Code.:

Synonyms:ethyl 4,6-O-benzylidene-2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 4,6-O-benzylidene-2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside

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Technology Process of ethyl 4,6-O-benzylidene-2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside

There total 6 articles about ethyl 4,6-O-benzylidene-2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 635684-80-9
ethyl 2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside

: 399035-88-2
ethyl 4,6-O-benzylidene-2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In N,N-dimethyl-formamide; at 70 ℃; for 2h;
DOI:10.1016/S0008-6215(01)00213-0

Reference yield:

: C₂₀H₂₈Cl₃NO₅SSi

: 399035-88-2
ethyl 4,6-O-benzylidene-2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201101267

Reference yield:

: 169557-88-4
ethyl-3,4,6-tri-O-acetyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamido)-1-thio-β-D-glucopyranoside

: 399035-88-2
ethyl 4,6-O-benzylidene-2-deoxy-2-N-trichloroacetamido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: MeONa / methanol / 3 h / 20 °C

2: (+/-)-camphor-10-sulfonic acid / dimethylformamide / 2 h / 70 °C

With camphor-10-sulfonic acid; sodium methylate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(01)00213-0