(E)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-propenyl>-1-<1-(2-<5-(1,3-dimethylhexahydro-2-oxo-1,3,5-triazinyl)>benzoyl)>cyclopentene

Base Information

Chemical Name:(E)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-propenyl>-1-<1-(2-<5-(1,3-dimethylhexahydro-2-oxo-1,3,5-triazinyl)>benzoyl)>cyclopentene
CAS No.:147806-16-4
Molecular Formula:C₃₀H₄₇N₃O₃Si
Molecular Weight:525.807
Hs Code.:

Synonyms:(E)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-propenyl>-1-<1-(2-<5-(1,3-dimethylhexahydro-2-oxo-1,3,5-triazinyl)>benzoyl)>cyclopentene

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Chemical Property of (E)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-propenyl>-1-<1-(2-<5-(1,3-dimethylhexahydro-2-oxo-1,3,5-triazinyl)>benzoyl)>cyclopentene

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Technology Process of (E)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-propenyl>-1-<1-(2-<5-(1,3-dimethylhexahydro-2-oxo-1,3,5-triazinyl)>benzoyl)>cyclopentene

There total 1 articles about (E)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-propenyl>-1-<1-(2-<5-(1,3-dimethylhexahydro-2-oxo-1,3,5-triazinyl)>benzoyl)>cyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 201230-82-2
carbon monoxide

: 130749-97-2
1,3-dimethyl-5-(2-iodophenyl)-hexahydro-2-oxo-1,3,5-triazine

: (E)-1-(trimethylstannyl)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-propenyl>cyclopentene

: 147806-16-4
(E)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-propenyl>-1-<1-(2-<5-(1,3-dimethylhexahydro-2-oxo-1,3,5-triazinyl)>benzoyl)>cyclopentene

Guidance literature:: With 1-methyl-pyrrolidin-2-one; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; lithium chloride; at 70 ℃; for 16h;

Reference yield: 87.0%

: 147806-16-4
(E)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-propenyl>-1-<1-(2-<5-(1,3-dimethylhexahydro-2-oxo-1,3,5-triazinyl)>benzoyl)>cyclopentene

: (+/-)-(1R*,2S*,4S*)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-(E)-propenyl>-1-<1-(2-<5-(1,3-dimethylhexahydro-2-oxo-1,3,5-triazinyl)>benzoyl)>-6-oxabicyclo<3.1.0>hexane

Guidance literature:: With tert.-butylhydroperoxide; N-benzyl-trimethylammonium hydroxide; In tetrahydrofuran; methanol; at -15 ℃; for 2h;

Reference yield:

: 147806-16-4
(E)-4-<1-(((triisopropylsilyl)oxy)methyl)-1-propenyl>-1-<1-(2-<5-(1,3-dimethylhexahydro-2-oxo-1,3,5-triazinyl)>benzoyl)>cyclopentene

: 5-(2-{1-[(1R,3R,5R)-3-((E)-1-Hydroxymethyl-propenyl)-6-oxa-bicyclo[3.1.0]hex-1-yl]-vinyl}-phenyl)-1,3-dimethyl-[1,3,5]triazinan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / tert-butylhydroperoxide, Triton B / tetrahydrofuran; methanol / 2 h / -15 °C

2: 91 percent / tetrahydrofuran / 4 h / Ambient temperature

3: 97 percent / n-Bu₄NF / tetrahydrofuran / 1 h / -15 °C

With tert.-butylhydroperoxide; tetrabutyl ammonium fluoride; N-benzyl-trimethylammonium hydroxide; In tetrahydrofuran; methanol;