tert-butyl (2S,3R)-3-phenylperoxyglycidate

Base Information

• Chemical Name: tert-butyl (2S,3R)-3-phenylperoxyglycidate
• CAS No.: 736141-00-7
• Molecular Formula: C₁₃H₁₆O₄
• Molecular Weight: 236.268

Synonyms:tert-butyl (2S,3R)-3-phenylperoxyglycidate

Chemical Property of tert-butyl (2S,3R)-3-phenylperoxyglycidate

Chemical Property:

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Technology Process of tert-butyl (2S,3R)-3-phenylperoxyglycidate

There total 11 articles about tert-butyl (2S,3R)-3-phenylperoxyglycidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert.-butylhydroperoxide (75-91-2) + 3-((E)-3-phenyl-2-propenoyl)-1,3-oxazolidin-2-one (109299-93-6) → (E)-tert-butyl 3-phenylprop-2-eneperoxoate (2123-92-4) + tert-butyl (2S,3R)-3-phenylperoxyglycidate (736141-00-7) + tert-butyl (2R,3S)-3-phenylperoxyglycidate (370084-23-4)

Guidance literature:

With La-(S)-BINOL-Ph₃AsO; 4 A molecular sieve; In tetrahydrofuran; toluene; at 20 ℃; for 4h; Title compound not separated from byproducts;

DOI:10.1016/j.tet.2003.06.010

Reference yield:

tert.-butylhydroperoxide (75-91-2) + cinnamoyl imidazole (1138-15-4,2979-51-3,30802-05-2) → (E)-tert-butyl 3-phenylprop-2-eneperoxoate (2123-92-4) + tert-butyl (2S,3R)-3-phenylperoxyglycidate (736141-00-7) + tert-butyl (2R,3S)-3-phenylperoxyglycidate (370084-23-4)

Guidance literature:

With La-(S)-BINOL-Ph₃AsO; 4 A molecular sieve; In tetrahydrofuran; toluene; at 20 ℃; for 4h; Title compound not separated from byproducts;

DOI:10.1016/j.tet.2003.06.010

Reference yield:

tert.-butylhydroperoxide (75-91-2) + cinnamoyl imidazole (1138-15-4,2979-51-3,30802-05-2) → tert-butyl (2S,3R)-3-phenylperoxyglycidate (736141-00-7) + tert-butyl (2R,3S)-3-phenylperoxyglycidate (370084-23-4)

Guidance literature:

With lanthanum(III) isopropoxide; 4 A molecular sieve; triphenylarsineoxide; (S)-[1,1']-binaphthalenyl-2,2'-diol; In tetrahydrofuran; decane; at 20 ℃; for 3.5h;

DOI:10.1021/ja0164879

upstream raw materials:

tert.-butylhydroperoxide

cinnamoyl imidazole

3-((E)-3-phenyl-2-propenoyl)-1,3-oxazolidin-2-one

4-methyl-1-[(2E)-1-oxo-3-phenyl-2-propenyl]-1H-imidazole

Downstream raw materials:

(S)-4-Methyl-2-[((2S,3R)-3-phenyl-oxiranecarbonyl)-amino]-pentanoic acid methyl ester

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