C₁₄H₁₇NOS

Base Information

• Chemical Name: C₁₄H₁₇NOS
• CAS No.: 1204834-83-2
• Molecular Formula: C₁₄H₁₇NOS
• Molecular Weight: 247.361
• Mol file: 1204834-83-2.mol

Synonyms:C₁₄H₁₇NOS

Chemical Property of C₁₄H₁₇NOS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₄H₁₇NOS

There total 2 articles about C₁₄H₁₇NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

3-methoxy-thiophene (17573-92-1) + methanol (67-56-1) + benzyl-methyl-amine (103-67-3) → C14H17NOS (1204834-83-2)

Guidance literature:

With [(N,N'-bis(diisopropylphosphino)-2,6-diaminopyridine)Mn(CO)₂H]; potassium tert-butylate; In toluene; at 130 ℃; for 16h; Inert atmosphere; Sealed tube; Green chemistry;

DOI:10.1021/jacs.7b05253

Reference yield: 60.0%

3-methoxy-thiophene (17573-92-1) + N,N'-dimethylbenzylamine (103-83-3) → C14H17NOS (1204834-83-2)

Guidance literature:

With pyridine N-oxide; [2,2]bipyridinyl; iron(II) chloride tetrahydrate; potassium iodide; In N,N-dimethyl acetamide; at 130 ℃; for 24h; Inert atmosphere;

DOI:10.1002/asia.200900157

upstream raw materials:

3-methoxy-thiophene

N,N'-dimethylbenzylamine

methanol

benzyl-methyl-amine