(3R)-(naphthalene-2-sulfonamido)-3-phenylpropionic acid tert-butyl ester

Base Information

Chemical Name:(3R)-(naphthalene-2-sulfonamido)-3-phenylpropionic acid tert-butyl ester
CAS No.:1190971-01-7
Molecular Formula:C₂₃H₂₅NO₄S
Molecular Weight:411.522
Hs Code.:

Synonyms:(3R)-(naphthalene-2-sulfonamido)-3-phenylpropionic acid tert-butyl ester

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Chemical Property of (3R)-(naphthalene-2-sulfonamido)-3-phenylpropionic acid tert-butyl ester

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Technology Process of (3R)-(naphthalene-2-sulfonamido)-3-phenylpropionic acid tert-butyl ester

There total 1 articles about (3R)-(naphthalene-2-sulfonamido)-3-phenylpropionic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 93-11-8
2-Naphthalenesulfonyl chloride

: 161671-34-7
tert-butyl (R)-3-amino-3-phenylpropionate

: 1190971-01-7
(3R)-(naphthalene-2-sulfonamido)-3-phenylpropionic acid tert-butyl ester

Guidance literature:: With triethylamine; dmap; In dichloromethane; at 20 ℃; Cooling with ice;

Reference yield: 100.0%

: 1190971-01-7
(3R)-(naphthalene-2-sulfonamido)-3-phenylpropionic acid tert-butyl ester

: 193634-01-4
(R)-3-(naphthalene-2-sulfonamido)-3-phenylpropanoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;

Reference yield:

: 1190971-01-7
(3R)-(naphthalene-2-sulfonamido)-3-phenylpropionic acid tert-butyl ester

: 1190970-05-8
(R)-N-(3-oxo-1-phenyl-3-(2-(piperidin-1-ylmethyl)-6,7-dihydrothieno[3,2-c]pyridin-5(4H)-yl)propyl)naphthalene-2-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 °C

2: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0 - 20 °C

With N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In dichloromethane;