(3-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)phenyl)diphenylphosphine oxide

Base Information

Chemical Name:(3-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)phenyl)diphenylphosphine oxide
CAS No.:328917-29-9
Molecular Formula:C₂₄H₂₆BO₃P
Molecular Weight:404.253
Hs Code.:

Synonyms:(3-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)phenyl)diphenylphosphine oxide

Suppliers and Price of (3-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)phenyl)diphenylphosphine oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)phenyl)diphenylphosphine oxide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of (3-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)phenyl)diphenylphosphine oxide

There total 7 articles about (3-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)phenyl)diphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 328917-28-8
2-[3-(diphenylphosphanyl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxoborolane

: 328917-29-9
(3-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)phenyl)diphenylphosphine oxide

Guidance literature:: With oxygen; potassium thioacyanate; iron(III) chloride; iodine; at 80 ℃; for 0.25h;
DOI:10.1002/1522-2675(20001108)83:11<2865::AID-HLCA2865>3.0.CO;2-A

Reference yield: 95.0%

: 10212-04-1
(3-bromophenyl)-diphenylphosphine oxide

: 73183-34-3
bis(pinacol)diborane

: 328917-29-9
(3-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)phenyl)diphenylphosphine oxide

Guidance literature:: With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; In 1,4-dioxane; for 12h; Reflux;

Reference yield:

: 108-36-1
1,3-dibromobenzene

: 328917-29-9
(3-(4,4,5,5-tetramethyl-1,3,2-dioxoborolan-2-yl)phenyl)diphenylphosphine oxide

Guidance literature:: Multi-step reaction with 4 steps

1.1: BuLi / tetrahydrofuran; hexane / 0.75 h / -90 °C

1.2: 90 percent / tetrahydrofuran; hexane / -90 - 20 °C

2.1: BuLi / tetrahydrofuran; hexane / 1 h / -90 °C

2.2: tetrahydrofuran; hexane / -90 - 20 °C

3.1: 43 percent / NH₄Cl / toluene / 2 h / Heating

4.1: 100 percent / FeCl₃*6H₂O; KSCN; O₂ / I₂ / 0.25 h / 80 °C

With n-butyllithium; oxygen; potassium thioacyanate; iron(III) chloride; ammonium chloride; iodine; In tetrahydrofuran; hexane; toluene;
DOI:10.1002/1522-2675(20001108)83:11<2865::AID-HLCA2865>3.0.CO;2-A