2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol

Base Information

Chemical Name:2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol
CAS No.:1356339-50-8
Molecular Formula:C₂₇H₃₆N₄O₃
Molecular Weight:464.608
Hs Code.:

Synonyms:2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol

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Chemical Property of 2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol

Chemical Property:

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Technology Process of 2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol

There total 3 articles about 2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.4%

: 62402-19-1
N-(2-methoxyethyl)-N-(pyridin-2-ylmethyl)amine

: 5862-32-8
2,6-bis(chloromethyl)-4-methylphenol

: 1356339-50-8
2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c1dt11187f

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 1356339-50-8
2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 0 - 20 °C

2: sodium tetrahydroborate / methanol / 0 °C

3: triethylamine / tetrahydrofuran; dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c1dt11187f

Reference yield:

: 150975-29-4
2-methoxy-N-((pyridin-2-yl)methylene)ethanamine

: 1356339-50-8
2,6-bis(((2-methoxyethyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 0 °C

2: triethylamine / tetrahydrofuran; dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c1dt11187f