Sb(C₆H₄Cl-m)3

Base Information

Chemical Name:Sb(C₆H₄Cl-m)3
CAS No.:24691-69-8
Molecular Formula:C₁₈H₁₂Cl₃Sb
Molecular Weight:456.402
Hs Code.:

Synonyms:Sb(C₆H₄Cl-m)3

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Chemical Property of Sb(C₆H₄Cl-m)3

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Technology Process of Sb(C₆H₄Cl-m)3

There total 1 articles about Sb(C₆H₄Cl-m)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 10025-91-9
antimony(III) chloride

: 36229-42-2
(3-chlorophenyl)magnesium bromide

: 24691-69-8
Sb(C₆H₄Cl-m)3

Guidance literature:: In diethyl ether; reacting at -12°C, then 1 h reflux; treating with aq. NH4Cl, evapn. ether layer, recrystn. from 95 % ethanol;
DOI:10.1021/ja01053a031

Reference yield: 74.0%

: 3102-33-8
trans-3-penten-2-one

: 24691-69-8
Sb(C₆H₄Cl-m)3

: 2050-67-1
PCB 11

: 4-(3-chlorophenyl)pentan-2-one

Guidance literature:: With silver(I) acetate; palladium diacetate; In acetic acid; at 25 ℃; for 24h;
DOI:10.1016/0040-4039(94)88042-5

Reference yield: 74.0%

: 3102-33-8
trans-3-penten-2-one

: 24691-69-8
Sb(C₆H₄Cl-m)3

: 4-(3-chlorophenyl)pentan-2-one

Guidance literature:: With palladium diacetate; silver(I) acetate; antimony(III) chloride; acetic acid; at 25 ℃; for 24h;
DOI:10.1246/bcsj.69.2341