C₃₂H₂₄N₂O₆

Base Information

Chemical Name:C₃₂H₂₄N₂O₆
CAS No.:1399266-36-4
Molecular Formula:C₃₂H₂₄N₂O₆
Molecular Weight:532.552
Hs Code.:

C<sub>32</sub>H<sub>24</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:C₃₂H₂₄N₂O₆

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Chemical Property of C₃₂H₂₄N₂O₆

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Technology Process of C₃₂H₂₄N₂O₆

There total 7 articles about C₃₂H₂₄N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1399266-33-1
C₃₂H₂₆N₂O₇

: 1399266-36-4
C₃₂H₂₄N₂O₆

Guidance literature:: C₃₂H₂₆N₂O₇; With diethylamino-sulfur trifluoride; In dichloromethane; at -78 ℃; for 5h; Inert atmosphere;

With potassium carbonate; In dichloromethane; at -78 - 22 ℃;
DOI:10.1039/c2ob26077h

Reference yield:

: 65-49-6
4-Aminosalicylic acid

: 1399266-36-4
C₃₂H₂₄N₂O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: sulfuric acid / 22 °C

2.1: acetic acid / 22 h / 118 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 22 °C / Inert atmosphere

4.1: potassium hydroxide; water / methanol / 18.5 h / 22 °C

5.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3.5 h / 22 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 22 °C / Inert atmosphere

7.1: diethylamino-sulfur trifluoride / dichloromethane / 5 h / -78 °C / Inert atmosphere

7.2: -78 - 22 °C

With oxalyl dichloride; diethylamino-sulfur trifluoride; sulfuric acid; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; potassium hydroxide; In methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26077h

Reference yield:

: 35019-69-3
4-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-2-hydroxy-benzoic acid methyl ester

: 1399266-36-4
C₃₂H₂₄N₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 22 °C / Inert atmosphere

2.1: potassium hydroxide; water / methanol / 18.5 h / 22 °C

3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3.5 h / 22 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 22 °C / Inert atmosphere

5.1: diethylamino-sulfur trifluoride / dichloromethane / 5 h / -78 °C / Inert atmosphere

5.2: -78 - 22 °C

With oxalyl dichloride; diethylamino-sulfur trifluoride; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; potassium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26077h