phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

Base Information

• Chemical Name: phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside
• CAS No.: 935268-61-4
• Molecular Formula: C₃₄H₂₇Cl₄NO₆S
• Molecular Weight: 719.469

Synonyms:phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

Chemical Property of phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

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Technology Process of phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

benzyl bromide (100-39-0) + phenyl 2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside (286018-83-5) → phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside (935268-61-4)

Guidance literature:

phenyl 2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside; With di(n-butyl)tin oxide; In toluene; for 12h; Heating;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In toluene; for 12h; Heating;

DOI:10.1021/ja069060g

Reference yield: 91.0%

phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside (935268-61-4) → phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside S-oxide (935268-64-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - -60 ℃; for 2h;

DOI:10.1021/ja069060g

Reference yield: 91.0%

phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside (935268-61-4) + t-butyldimethylsiyl triflate (69739-34-0) → phenyl 2-deoxy-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside (935268-62-5)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at 20 ℃;

DOI:10.1021/ja069060g

upstream raw materials:

benzyl bromide

phenyl 2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

Downstream raw materials:

phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside S-oxide

phenyl 2-deoxy-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

phenyl 2-deoxy-3,6-di-O-benzyl-4-O-tert-butyldimethylsilyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside S-oxide

phenyl 2-deoxy-3,6-di-O-benzyl-2-tetrachlorophthalimido-β-D-glucopyranosyl-(1->4)-2-deoxy-6-O-benzyl-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

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