o-tolyl methyl ketene

Base Information

Chemical Name:o-tolyl methyl ketene
CAS No.:945666-91-1
Molecular Formula:C₁₀H₁₀O
Molecular Weight:146.189
Hs Code.:

Synonyms:o-tolyl methyl ketene

Suppliers and Price of o-tolyl methyl ketene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-tolyl methyl ketene

Chemical Property:

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Technology Process of o-tolyl methyl ketene

There total 1 articles about o-tolyl methyl ketene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137144-15-1,144789-13-9,62835-95-4
(rac)-2-(2-methylphenyl)propanoic acid

: 945666-91-1
o-tolyl methyl ketene

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / toluene / 12 h / 20 - 80 °C

2: SEC-BUTYLAMINE / tetrahydrofuran / 0 °C / Inert atmosphere

With thionyl chloride; SEC-BUTYLAMINE; In tetrahydrofuran; toluene;
DOI:10.1002/chem.201503308

Reference yield: 97.0%

: 945666-91-1
o-tolyl methyl ketene

: Z-3-methyl-3-o-tolyl-4-(1-o-tolylethylidene)oxetan-2-one

Guidance literature:: With tributylphosphine; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2020.131838

Reference yield: 93.0%

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 945666-91-1
o-tolyl methyl ketene

: C₁₆H₁₉NO

Guidance literature:: With C₄₅H₃₁O₄P; In 1,2-dichloro-ethane; at 20 ℃; for 30h; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1039/d1cc05307h