methyl endo,endo-6-bromo-7-hydroxy-7-phenylbicyclo<3.1.1>heptane-6-carboxylate

Base Information

Chemical Name:methyl endo,endo-6-bromo-7-hydroxy-7-phenylbicyclo<3.1.1>heptane-6-carboxylate
CAS No.:340703-63-1
Molecular Formula:C₁₅H₁₇BrO₃
Molecular Weight:325.202
Hs Code.:

Synonyms:methyl endo,endo-6-bromo-7-hydroxy-7-phenylbicyclo<3.1.1>heptane-6-carboxylate

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Chemical Property of methyl endo,endo-6-bromo-7-hydroxy-7-phenylbicyclo<3.1.1>heptane-6-carboxylate

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Technology Process of methyl endo,endo-6-bromo-7-hydroxy-7-phenylbicyclo<3.1.1>heptane-6-carboxylate

There total 3 articles about methyl endo,endo-6-bromo-7-hydroxy-7-phenylbicyclo<3.1.1>heptane-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 67-56-1
methanol

: 129576-93-8
6-bromo-7-phenylbicyclo<3.1.1>heptane-6,7-carbolactone

: 340703-63-1
methyl endo,endo-6-bromo-7-hydroxy-7-phenylbicyclo<3.1.1>heptane-6-carboxylate

Guidance literature:: With sulfuric acid; Ambient temperature;

Reference yield:

: 57293-39-7
1-Phenyltricyclo<4.1.0.0.^2,7>heptane

: 340703-63-1
methyl endo,endo-6-bromo-7-hydroxy-7-phenylbicyclo<3.1.1>heptane-6-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) butyllithium, tetramethylethylenediamine / 1.) ether, from 0 deg C to RT, 12 h, 2.) ether

2: 75 percent / N-bromosuccinimide / tetrahydrofuran / 5 h / 20 °C

3: 72 percent / H₂SO₄ / Ambient temperature

With N-Bromosuccinimide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; In tetrahydrofuran;

Reference yield:

: 129576-92-7
7-phenyltricyclo<4.1.0.0^2,7>heptane-1-carboxylic acid

: 340703-63-1
methyl endo,endo-6-bromo-7-hydroxy-7-phenylbicyclo<3.1.1>heptane-6-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / N-bromosuccinimide / tetrahydrofuran / 5 h / 20 °C

2: 72 percent / H₂SO₄ / Ambient temperature

With N-Bromosuccinimide; sulfuric acid; In tetrahydrofuran;