(S)-methyl 2-(benzoylamino)-6-(((tert-butyloxy)carbonyl)amino)hexanoate

Base Information

Chemical Name:(S)-methyl 2-(benzoylamino)-6-(((tert-butyloxy)carbonyl)amino)hexanoate
CAS No.:331714-14-8
Molecular Formula:C₁₉H₂₈N₂O₅
Molecular Weight:364.442
Hs Code.:

Synonyms:(S)-methyl 2-(benzoylamino)-6-(((tert-butyloxy)carbonyl)amino)hexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 2-(benzoylamino)-6-(((tert-butyloxy)carbonyl)amino)hexanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of (S)-methyl 2-(benzoylamino)-6-(((tert-butyloxy)carbonyl)amino)hexanoate

There total 1 articles about (S)-methyl 2-(benzoylamino)-6-(((tert-butyloxy)carbonyl)amino)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 98-88-4
benzoyl chloride

: 2389-48-2
N-ε-tert-butoxycarbonyl-L-lysine methyl ester hydrochloride

: 331714-14-8
(S)-methyl 2-(benzoylamino)-6-(((tert-butyloxy)carbonyl)amino)hexanoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25 ℃; for 1h;
DOI:10.1021/ja003579+

Reference yield:

: 331714-14-8
(S)-methyl 2-(benzoylamino)-6-(((tert-butyloxy)carbonyl)amino)hexanoate

: 14280-01-4
(2S)-N^α-benzoyllysine methyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 25 ℃; for 3h;
DOI:10.1021/ja003579+

Reference yield:

: 331714-14-8
(S)-methyl 2-(benzoylamino)-6-(((tert-butyloxy)carbonyl)amino)hexanoate

: 331714-15-9
(S)-methyl 2-(benzoylamino)-6-[2-(((tert-butyloxy)carbonyl)amino)-acetamido]hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / dioxane; CH₂Cl₂ / 3 h / 25 °C

2: PyBrOP; i-Pr₂NEt / dimethylformamide / 12 h / 25 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja003579+