1-S-acetyl-2,6-anhydro-1-deoxy-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol

Base Information

Chemical Name:1-S-acetyl-2,6-anhydro-1-deoxy-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol
CAS No.:199784-03-7
Molecular Formula:C₃₇H₄₀O₆S
Molecular Weight:612.787
Hs Code.:

Synonyms:1-S-acetyl-2,6-anhydro-1-deoxy-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-S-acetyl-2,6-anhydro-1-deoxy-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol

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Technology Process of 1-S-acetyl-2,6-anhydro-1-deoxy-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol

There total 3 articles about 1-S-acetyl-2,6-anhydro-1-deoxy-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: Methanesulfonic acid (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-ylmethyl ester

: 10387-40-3
potassium thioacetate

: 199784-03-7
1-S-acetyl-2,6-anhydro-1-deoxy-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol

Guidance literature:: In ethanol; for 16h; Heating;
DOI:10.1021/ol0502127 DOI:10.1021/jm050422p

Reference yield: 83.0%

: 133697-34-4,97321-70-5
2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-deoxy-D-gluco-hept-1-enitol

: 507-09-5
tiolacetic acid

: 199784-03-7
1-S-acetyl-2,6-anhydro-1-deoxy-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In benzene; for 4h; Heating;
DOI:10.1016/S0040-4020(97)01021-1

Reference yield:

: 89064-71-1
β-C-(hydroxymethyl)-2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

: 199784-03-7
1-S-acetyl-2,6-anhydro-1-deoxy-3,4,5,7-tetra-O-benzyl-D-glycero-D-gulo-heptitol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / pyridine / CH₂Cl₂ / 2.5 h

2: 92 percent / ethanol / 16 h / Heating

With pyridine; In ethanol; dichloromethane;
DOI:10.1021/ol0502127 DOI:10.1021/jm050422p