(C6H-2,6-(C6H2-2,4,6-(i)Pr3)2-3,5-(i)Pr2)Co(η6-toluene)

Base Information

Chemical Name:(C6H-2,6-(C6H2-2,4,6-(i)Pr3)2-3,5-(i)Pr2)Co(η6-toluene)
CAS No.:1076223-27-2
Molecular Formula:C₄₉H₆₉Co
Molecular Weight:717.08
Hs Code.:

Synonyms:(C6H-2,6-(C6H2-2,4,6-(i)Pr3)2-3,5-(i)Pr2)Co(η6-toluene)

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Chemical Property of (C6H-2,6-(C6H2-2,4,6-(i)Pr3)2-3,5-(i)Pr2)Co(η6-toluene)

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Technology Process of (C6H-2,6-(C6H2-2,4,6-(i)Pr3)2-3,5-(i)Pr2)Co(η6-toluene)

There total 1 articles about (C6H-2,6-(C6H2-2,4,6-(i)Pr3)2-3,5-(i)Pr2)Co(η6-toluene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 110-54-3
hexane

: [(C6H-2,6-(C6H2-2,4,6-(i)Pr3)2-3,5-(i)Pr2)Co(μ-Cl)]2

: 108-88-3,15644-74-3,16713-13-6
toluene

: 1076223-27-2
(C6H-2,6-(C6H2-2,4,6-(i)Pr3)2-3,5-(i)Pr2)Co(η6-toluene)

Guidance literature:: With KC₈; In toluene; a soln. of Co complex added to a suspn. of KC8 at 0°C, stirred for ca 24 h; evapd. (vac.), extd. (hexane), filtered, concd., crystd. at -18°Cfor 1 d; elem. anal.;
DOI:10.1021/ic8015782

Reference yield: 38.0%

: 110-54-3
hexane

: 1076223-27-2
(C6H-2,6-(C6H2-2,4,6-(i)Pr3)2-3,5-(i)Pr2)Co(η6-toluene)

: 80937-33-3
oxygen

: C₈₄H₁₂₂Co₂O₄*2.5C₆H₁₄

Guidance literature:: at 25 ℃; for 1.5h; under 760.051 Torr; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.inorgchem.5b00930

Reference yield: 32.0%

: 1076223-27-2
(C6H-2,6-(C6H2-2,4,6-(i)Pr3)2-3,5-(i)Pr2)Co(η6-toluene)

: 201230-82-2
carbon monoxide

: (C₆H-2,6-(C₆H₂-2,4,6-(i)Pr₃)2-3,5-(i)Pr₂)C(O)Co(CO)

Guidance literature:: In diethyl ether; a soln. of Co complex treated with CO (1 atm) at room temp. for 2 h, stirred for ca 24 h; evapd. (vac.), extd. (hexane), crystd. for days at -18°C; elem. anal.;
DOI:10.1021/ic8015782