5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carbaldehyde

Base Information

Chemical Name:5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carbaldehyde
CAS No.:1041857-78-6
Molecular Formula:C₂₀H₁₆O₄S
Molecular Weight:352.411
Hs Code.:

Synonyms:5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carbaldehyde

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Chemical Property of 5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carbaldehyde

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Technology Process of 5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carbaldehyde

There total 1 articles about 5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1041857-76-4
2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1041857-78-6
5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carbaldehyde

Guidance literature:: 2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -50 ℃; for 2h;

With water; ammonium chloride; In tetrahydrofuran; hexane; Further stages.;
DOI:10.1016/j.bmc.2008.04.009

Reference yield:

: 1041857-78-6
5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carbaldehyde

: 506-59-2
N,N-dimethylammonium chloride

: C₂₂H₂₃NO₃S

Guidance literature:: 5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carbaldehyde; N,N-dimethylammonium chloride; With titanium(IV) isopropylate; triethylamine; In ethanol; at 20 ℃; for 20h;

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 5.5h; Further stages.;
DOI:10.1016/j.bmc.2008.04.009