2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane

Base Information

Chemical Name:2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane
CAS No.:1041857-76-4
Molecular Formula:C₁₉H₁₆O₃S
Molecular Weight:324.4
Hs Code.:

Synonyms:2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane

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Chemical Property of 2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane

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Technology Process of 2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane

There total 1 articles about 2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 107-21-1
ethylene glycol

: 848642-00-2
3-{4-[2-(methoxymethyl)phenyl]buta-1,3-diynyl}thiophene-2-carbaldehyde

: 1041857-76-4
2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane

Guidance literature:: With pyridinium p-toluenesulfonate; In benzene; for 37h; Heating;
DOI:10.1016/j.bmc.2008.04.009

Reference yield: 88.0%

: 1041857-76-4
2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1041857-78-6
5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carbaldehyde

Guidance literature:: 2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -50 ℃; for 2h;

With water; ammonium chloride; In tetrahydrofuran; hexane; Further stages.;
DOI:10.1016/j.bmc.2008.04.009

Reference yield: 80.0%

: 1041857-76-4
2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane

: 79-22-1
methyl chloroformate

: 1041857-81-1
5-[1,3]dioxolan-2-yl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid methyl ester

Guidance literature:: 2-{3-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-[1,3]dioxolane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

methyl chloroformate; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Further stages.;
DOI:10.1016/j.bmc.2008.04.009