1,1-dimethyl-2,2,2-trichloroethyl 5'-O-momo-p-methoxytritylthymidyl-3' thymidyl-5 phosphite

Base Information

Chemical Name:1,1-dimethyl-2,2,2-trichloroethyl 5'-O-momo-p-methoxytritylthymidyl-3' thymidyl-5 phosphite
CAS No.:90813-75-5
Molecular Formula:C₄₄H₄₈Cl₃N₄O₁₂P
Molecular Weight:962.217
Hs Code.:

Synonyms:1,1-dimethyl-2,2,2-trichloroethyl 5'-O-momo-p-methoxytritylthymidyl-3' thymidyl-5 phosphite

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-dimethyl-2,2,2-trichloroethyl 5'-O-momo-p-methoxytritylthymidyl-3' thymidyl-5 phosphite

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Technology Process of 1,1-dimethyl-2,2,2-trichloroethyl 5'-O-momo-p-methoxytritylthymidyl-3' thymidyl-5 phosphite

There total 1 articles about 1,1-dimethyl-2,2,2-trichloroethyl 5'-O-momo-p-methoxytritylthymidyl-3' thymidyl-5 phosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 39177-74-7
2,2,2-trichloro-1,1-dimethylethyldichloro phosphite

: 42926-80-7
5'-O-(4-monomethoxytrityl)-2'-deoxythymidine

: 65-71-4,28806-14-6,691841-57-3
thymin

: 90813-75-5
1,1-dimethyl-2,2,2-trichloroethyl 5'-O-momo-p-methoxytritylthymidyl-3' thymidyl-5 phosphite

Guidance literature:: In tetrahydrofuran; pyridine; 1.) -78 deg C, 15 min; 2.) -78 deg C, 15 min, warmed to 0 deg C over 15 min;
DOI:10.1016/0040-4020(84)85112-1