4-Nitrobenzyl (1R,5S,6S)-2-(2-diethylcarbamoyl-phenylsulphinyl)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate

Base Information

• Chemical Name: 4-Nitrobenzyl (1R,5S,6S)-2-(2-diethylcarbamoyl-phenylsulphinyl)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate
• CAS No.: 158250-79-4
• Molecular Formula: C₂₈H₃₁N₃O₈S
• Molecular Weight: 569.635

Synonyms:4-Nitrobenzyl (1R,5S,6S)-2-(2-diethylcarbamoyl-phenylsulphinyl)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate

Chemical Property of 4-Nitrobenzyl (1R,5S,6S)-2-(2-diethylcarbamoyl-phenylsulphinyl)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate

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Technology Process of 4-Nitrobenzyl (1R,5S,6S)-2-(2-diethylcarbamoyl-phenylsulphinyl)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate

There total 4 articles about 4-Nitrobenzyl (1R,5S,6S)-2-(2-diethylcarbamoyl-phenylsulphinyl)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

4-nitrobenzyl (1 R ,5 S ,6 S)-2-(2-diethylcarbamoylphenylthio)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate (158168-60-6) → 4-Nitrobenzyl (1R,5S,6S)-2-(2-diethylcarbamoyl-phenylsulphinyl)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate (158250-79-4)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; sodium sulfite;

Reference yield: 25.0%

4-nitrobenzyl (1 R ,5 S ,6 S)-2-(2-diethylcarbamoylphenylthio)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate (158168-60-6) + sodium sulfite (7757-83-7) → 4-Nitrobenzyl (1R,5S,6S)-2-(2-diethylcarbamoyl-phenylsulphinyl)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate (158250-79-4)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;

Reference yield:

bromomagnesium isopropylcyclohexylamide + 4-nitrobenzyl 2-(dimethylcarbamoyl)-4-mercaptopyrrolidine-1-carboxylate → 4-Nitrobenzyl (1R,5S,6S)-2-(2-diethylcarbamoyl-phenylsulphinyl)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate (158250-79-4)

Guidance literature:

In tetrahydrofuran;

upstream raw materials:

4-nitrobenzyl (1 R ,5 S ,6 S)-2-(2-diethylcarbamoylphenylthio)-1-methyl-6-[1(R)-hydroxyethyl]-1-carbapen-2-em-3-carboxylate

3-chloro-benzenecarboperoxoic acid

sodium sulfite

Downstream raw materials:

4-Nitrobenzyl (1R,5S,6S)-2-{(3S,5S)-5-[3(S)-(4-nitrobenzyloxycarbonyl)aminopyrrolidin-1-ylcarbonyl]-1-methylpyrrolidin-3-ylthio}-6-[1(R)-hydroxyethyl]-1-methyl-1-carbapen-2-em-3-carboxylate

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