Morpholine-4-carbothioic acid ((Z)-1-phenyl-3-pyrrolidin-1-yl-3-thioxo-propenyl)-amide

Base Information

Chemical Name:Morpholine-4-carbothioic acid ((Z)-1-phenyl-3-pyrrolidin-1-yl-3-thioxo-propenyl)-amide
CAS No.:118200-13-8
Molecular Formula:C₁₈H₂₃N₃OS₂
Molecular Weight:361.532
Hs Code.:

Synonyms:Morpholine-4-carbothioic acid ((Z)-1-phenyl-3-pyrrolidin-1-yl-3-thioxo-propenyl)-amide

Suppliers and Price of Morpholine-4-carbothioic acid ((Z)-1-phenyl-3-pyrrolidin-1-yl-3-thioxo-propenyl)-amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Morpholine-4-carbothioic acid ((Z)-1-phenyl-3-pyrrolidin-1-yl-3-thioxo-propenyl)-amide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Morpholine-4-carbothioic acid ((Z)-1-phenyl-3-pyrrolidin-1-yl-3-thioxo-propenyl)-amide

There total 8 articles about Morpholine-4-carbothioic acid ((Z)-1-phenyl-3-pyrrolidin-1-yl-3-thioxo-propenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 123-75-1
pyrrolidine

: 70757-27-6
2-morpholin-4-yl-4-phenyl-[1,3]thiazine-6-thione

: 118200-13-8
Morpholine-4-carbothioic acid ((Z)-1-phenyl-3-pyrrolidin-1-yl-3-thioxo-propenyl)-amide

Guidance literature:: In methanol; for 0.5h; Heating;
DOI:10.1007/BF00810427

Reference yield:

: 2-Morpholino-6-pyrrolidino-4-phenyl-1,3-thiazinium-perchlorat

: 118200-13-8
Morpholine-4-carbothioic acid ((Z)-1-phenyl-3-pyrrolidin-1-yl-3-thioxo-propenyl)-amide

Guidance literature:: With hydrogen sulfide; triethylamine; In acetonitrile; for 0.333333h; Heating;
DOI:10.1007/BF00810427

Reference yield:

: 118200-24-1
4-Phenyl-6-pyrrolidino-1,3-thiazin-2-thion

: 118200-13-8
Morpholine-4-carbothioic acid ((Z)-1-phenyl-3-pyrrolidin-1-yl-3-thioxo-propenyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / 2) 70percent HClO₄/glacial acetic acid / benzene / 0.25 h / Heating

2: 71 percent / acetonitrile / 48 h / Ambient temperature

3: NEt₃, H₂S / acetonitrile / 0.33 h / Heating

With perchloric acid; hydrogen sulfide; acetic acid; triethylamine; In acetonitrile; benzene;
DOI:10.1007/BF00810427