methyl 3-cyano-4-fluoro-N-(trimethylsilylmethyl)benzenecarboximidothioate

Base Information

Chemical Name:methyl 3-cyano-4-fluoro-N-(trimethylsilylmethyl)benzenecarboximidothioate
CAS No.:1256832-38-8
Molecular Formula:C₁₃H₁₇FN₂SSi
Molecular Weight:280.441
Hs Code.:

Synonyms:methyl 3-cyano-4-fluoro-N-(trimethylsilylmethyl)benzenecarboximidothioate

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Chemical Property of methyl 3-cyano-4-fluoro-N-(trimethylsilylmethyl)benzenecarboximidothioate

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Technology Process of methyl 3-cyano-4-fluoro-N-(trimethylsilylmethyl)benzenecarboximidothioate

There total 5 articles about methyl 3-cyano-4-fluoro-N-(trimethylsilylmethyl)benzenecarboximidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1256832-30-0
3-cyano-4-fluoro-N-(trimethylsilylmethyl)benzenecarbothioamide

: 74-88-4
methyl iodide

: 1256832-38-8
methyl 3-cyano-4-fluoro-N-(trimethylsilylmethyl)benzenecarboximidothioate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield:

: 1174731-61-3
3-bromo-4-fluoro-N-(trimethylsilylmethyl)benzamide

: 1256832-38-8
methyl 3-cyano-4-fluoro-N-(trimethylsilylmethyl)benzenecarboximidothioate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 4 - 5 h / 100 °C / Sealed tube; Inert atmosphere

2: Lawessons reagent / tetrahydrofuran / 2 h / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

With Lawessons reagent; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 1007-16-5
3-bromo-4-fluorobenzoic acid

: 1256832-38-8
methyl 3-cyano-4-fluoro-N-(trimethylsilylmethyl)benzenecarboximidothioate

Guidance literature:: Multi-step reaction with 4 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 4 - 5 h / 100 °C / Sealed tube; Inert atmosphere

3: Lawessons reagent / tetrahydrofuran / 2 h / Reflux

4: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

With Lawessons reagent; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;