methyl propargyl ether, dicobalt-hexacarbonyl complex

Base Information

Chemical Name:methyl propargyl ether, dicobalt-hexacarbonyl complex
CAS No.:65966-21-4
Molecular Formula:C₁₀H₆Co₂O₇
Molecular Weight:356.14
Hs Code.:

Synonyms:methyl propargyl ether, dicobalt-hexacarbonyl complex

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Chemical Property of methyl propargyl ether, dicobalt-hexacarbonyl complex

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Technology Process of methyl propargyl ether, dicobalt-hexacarbonyl complex

There total 2 articles about methyl propargyl ether, dicobalt-hexacarbonyl complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (μ-propylbutenolide)-(μ-CO)Co2(CO)6

: 627-41-8
propargyl alcohol methyl ether

: 65966-21-4
methyl propargyl ether, dicobalt-hexacarbonyl complex

: (C₄O₂HC₃H₇)(HC₂C₆H₅)2Co₂(CO)5

: (C₄O₂HC₃H₇)(HC₂CH₂OCH₃)2Co₂(CO)5

Guidance literature:: With carbon monoxide; hydroquinone; In benzene; A soln. of reagents in benzene was kept under CO at 25°C, the mixt. was stirred for 2-3 h;; filtered, chromd. on silica TLC plates with CH2Cl2, Et2O, repeated chromy. on TLC and/or twofold recrystd. from n-hexane;;
DOI:10.1016/S0022-328X(00)93470-3

Reference yield:

: (μ-phenylbutenolide)-(μ-CO)Co2(CO)6

: 627-41-8
propargyl alcohol methyl ether

: 65966-21-4
methyl propargyl ether, dicobalt-hexacarbonyl complex

: (C₄O₂HC₆H₅)(HC₂CH₂OCH₃)2Co₂(CO)5

: (C₄O₂HC₆H₅)(HC₂CH₂OCH₃)2Co₂(CO)5

Guidance literature:: With carbon monoxide; hydroquinone; In benzene; A soln. of reagents in benzene was kept under CO at 25°C, the mixt. was stirred for 2-3 h;; filtered, chromd. on silica TLC plates with CH2Cl2, Et2O, repeated chromy. on TLC and/or twofold recrystd. from n-hexane; elem. anal.;;
DOI:10.1016/S0022-328X(00)93470-3

Reference yield: 92.0%

: 65966-21-4
methyl propargyl ether, dicobalt-hexacarbonyl complex

: 6651-36-1
1-(Trimethylsilyloxy)cyclohexene

: 73969-85-4
Co₂(CO)6C₆H₉OCH₂CCH

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; BF3*OEt2, CH2Cl2, -78°C; chromy. on silica gel;
DOI:10.1021/ja00271a066