6-((S)-2,4,6-Triisopropyl-benzenesulfinyl)-1,4-dioxa-spiro[4.4]non-6-ene

Base Information

Chemical Name:6-((S)-2,4,6-Triisopropyl-benzenesulfinyl)-1,4-dioxa-spiro[4.4]non-6-ene
CAS No.:198342-53-9
Molecular Formula:C₂₂H₃₂O₃S
Molecular Weight:376.56
Hs Code.:

Synonyms:6-((S)-2,4,6-Triisopropyl-benzenesulfinyl)-1,4-dioxa-spiro[4.4]non-6-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-((S)-2,4,6-Triisopropyl-benzenesulfinyl)-1,4-dioxa-spiro[4.4]non-6-ene

Chemical Property:

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Technology Process of 6-((S)-2,4,6-Triisopropyl-benzenesulfinyl)-1,4-dioxa-spiro[4.4]non-6-ene

There total 3 articles about 6-((S)-2,4,6-Triisopropyl-benzenesulfinyl)-1,4-dioxa-spiro[4.4]non-6-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 198342-53-9
6-((S)-2,4,6-Triisopropyl-benzenesulfinyl)-1,4-dioxa-spiro[4.4]non-6-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / Zn / H₂O / 1 h / 90 °C

2: 1.) SOCl₂, 2.) pyridine / 1.) room temp., 3.5 h, 2.) Et₂O, room temp., overnight

3: 1.) n-BuLi / 1.) THF, -100 deg C, 20 min, 2.) THF, -100 deg C, 30 min

With pyridine; n-butyllithium; thionyl chloride; zinc; In water;
DOI:10.1021/jo971093e

Reference yield:

: 717-74-8
1,3,5-triisopropyl benzene

: 198342-53-9
6-((S)-2,4,6-Triisopropyl-benzenesulfinyl)-1,4-dioxa-spiro[4.4]non-6-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / ClSO₃H / CHCl₃ / 0 °C

2: 69 percent / Zn / H₂O / 1 h / 90 °C

3: 1.) SOCl₂, 2.) pyridine / 1.) room temp., 3.5 h, 2.) Et₂O, room temp., overnight

4: 1.) n-BuLi / 1.) THF, -100 deg C, 20 min, 2.) THF, -100 deg C, 30 min

With pyridine; chlorosulfonic acid; n-butyllithium; thionyl chloride; zinc; In chloroform; water;
DOI:10.1021/jo971093e

Reference yield:

: 68241-78-1
6-bromo-1,4-dioxa-spiro[4.4]non-6-ene

: 198342-81-3
S_S-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate

: 198342-53-9
6-((S)-2,4,6-Triisopropyl-benzenesulfinyl)-1,4-dioxa-spiro[4.4]non-6-ene

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, -100 deg C, 20 min, 2.) THF, -100 deg C, 30 min;
DOI:10.1021/jo971093e