3-(benzyloxycarbonylamino)propylammonium trifluoroacetate

Base Information

Chemical Name:3-(benzyloxycarbonylamino)propylammonium trifluoroacetate
CAS No.:1192134-66-9
Molecular Formula:C₂HF₃O₂*C₁₁H₁₆N₂O₂
Molecular Weight:322.284
Hs Code.:

Synonyms:3-(benzyloxycarbonylamino)propylammonium trifluoroacetate

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Chemical Property of 3-(benzyloxycarbonylamino)propylammonium trifluoroacetate

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Technology Process of 3-(benzyloxycarbonylamino)propylammonium trifluoroacetate

There total 1 articles about 3-(benzyloxycarbonylamino)propylammonium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 160291-51-0
N-(tert-butoxycarbonyl)-N'-(benzyloxycarbonyl)-1,3-propanediamine

: 76-05-1
trifluoroacetic acid

: 1192134-66-9
3-(benzyloxycarbonylamino)propylammonium trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 2h;
DOI:10.3184/174751916X14792878808106

Reference yield: 79.0%

: 75-44-5
phosgene

: 1192134-66-9
3-(benzyloxycarbonylamino)propylammonium trifluoroacetate

: 872060-34-9
3-(benzyloxycarbonylamino)propyl isocyanate

Guidance literature:: 3-(benzyloxycarbonylamino)propylammonium trifluoroacetate; In dichloromethane; water; at 0 ℃; for 0.5h;

phosgene; In dichloromethane; at 20 ℃; Cooling with ice;
DOI:10.3184/174751916X14792878808106

Reference yield: 71.0%

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1192134-66-9
3-(benzyloxycarbonylamino)propylammonium trifluoroacetate

: 1192134-59-0
(S)-2-(3-benzyloxycarbonylaminopropylcarbamoyl)pyrrolidine-1-carboxylic acid tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; for 17h; Inert atmosphere;
DOI:10.1055/s-0029-1216885