N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-(N,N-diisobutylamino)ethylsulfonamide

Base Information

Chemical Name:N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-(N,N-diisobutylamino)ethylsulfonamide
CAS No.:1381785-17-6
Molecular Formula:C₂₇H₃₄F₆N₄O₃S
Molecular Weight:608.648
Hs Code.:

Synonyms:N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-(N,N-diisobutylamino)ethylsulfonamide

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Chemical Property of N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-(N,N-diisobutylamino)ethylsulfonamide

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Technology Process of N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-(N,N-diisobutylamino)ethylsulfonamide

There total 5 articles about N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-(N,N-diisobutylamino)ethylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 110-96-3
diisobutylamine

: 1381785-83-6
N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-bromoethylsulfonamide

: 1381785-17-6
N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-(N,N-diisobutylamino)ethylsulfonamide

Guidance literature:: In acetonitrile; at 80 ℃; for 18h;

Reference yield:

: 1736-74-9
4-trifluoromethoxybenzyl alcohol

: 1381785-17-6
N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-(N,N-diisobutylamino)ethylsulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 1 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

2.2: 0 °C

3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 - 20 °C

4.1: acetonitrile / 18 h / 80 °C

With lithium aluminium tetrahydride; carbon tetrabromide; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 1381785-80-3
Methyl N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate

: 1381785-17-6
N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-(N,N-diisobutylamino)ethylsulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 1 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

2.2: 0 °C

3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 - 20 °C

4.1: acetonitrile / 18 h / 80 °C

With lithium aluminium tetrahydride; carbon tetrabromide; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;