Methyl N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate

Base Information

Chemical Name:Methyl N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate
CAS No.:1381785-80-3
Molecular Formula:C₁₂H₁₂F₃N₃O₄S
Molecular Weight:351.306
Hs Code.:

Synonyms:Methyl N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate

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Technology Process of Methyl N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate

There total 1 articles about Methyl N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 56146-83-9
chlorosulfonyl-acetic acid methyl ester

: 1381785-79-0
2-Amino-7-trifluoromethyl-3-methylimidazo[1,2-a]pyridine hydrochloride

: 1381785-80-3
Methyl N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 100.0%

: 1736-74-9
4-trifluoromethoxybenzyl alcohol

: 1381785-80-3
Methyl N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate

: 1381785-81-4
Methyl N-(4-trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 1381785-80-3
Methyl N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)sulfamoylacetate

: 1381785-82-5
N-(4-Trifluoromethoxybenzyl)-N-(7-trifluoromethyl-3-methylimidazo[1,2-a]pyridin-2-yl)-2-hydroxyethylsulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 1 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

2.2: 0 °C

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran;