(E)-2-(2,4,6-trimethylphenyl)methylenecyclobutanone

Base Information

Chemical Name:(E)-2-(2,4,6-trimethylphenyl)methylenecyclobutanone
CAS No.:1520990-20-8
Molecular Formula:C₁₄H₁₆O
Molecular Weight:200.28
Hs Code.:

Synonyms:(E)-2-(2,4,6-trimethylphenyl)methylenecyclobutanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(2,4,6-trimethylphenyl)methylenecyclobutanone

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Technology Process of (E)-2-(2,4,6-trimethylphenyl)methylenecyclobutanone

There total 1 articles about (E)-2-(2,4,6-trimethylphenyl)methylenecyclobutanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 487-68-3
mesytaldehyde

: 1191-95-3
cyclobutanone

: 1520990-20-8
(E)-2-(2,4,6-trimethylphenyl)methylenecyclobutanone

Guidance literature:: With calcium hydroxide; In ethanol; at 80 ℃; for 24h; stereoselective reaction; Inert atmosphere; Green chemistry;
DOI:10.1039/c3gc41562g

Reference yield: 53.0%

: 1520990-20-8
(E)-2-(2,4,6-trimethylphenyl)methylenecyclobutanone

: (E)-2-(2,4,6-trimethylbenzylidene)cyclobutan-1-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 4h;
DOI:10.1016/j.tet.2019.130563

Reference yield:

: 1520990-20-8
(E)-2-(2,4,6-trimethylphenyl)methylenecyclobutanone

: (E)-2-(2,4,6-trimethylbenzylidene)cyclobutan-1-ol

: (R,E)-2-(2,4,6-trimethylbenzylidene)cyclobutan-1-ol

Guidance literature:: With C₈₄H₈₀Cl₄N₂O₂P₄Ru₃; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; at 20 ℃; for 1h; under 1500.15 Torr; Overall yield = 96 %; Overall yield = 58.3 mg; enantioselective reaction; Autoclave;
DOI:10.1021/acs.orglett.9b01514