(N-Benzyl-norcodeinondimethylacetal-14-yl)-β-dimethylaminoethan

Base Information

Chemical Name:(N-Benzyl-norcodeinondimethylacetal-14-yl)-β-dimethylaminoethan
CAS No.:145221-14-3
Molecular Formula:C₃₀H₃₈N₂O₄
Molecular Weight:490.643
Hs Code.:

Synonyms:(N-Benzyl-norcodeinondimethylacetal-14-yl)-β-dimethylaminoethan

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Chemical Property of (N-Benzyl-norcodeinondimethylacetal-14-yl)-β-dimethylaminoethan

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Technology Process of (N-Benzyl-norcodeinondimethylacetal-14-yl)-β-dimethylaminoethan

There total 7 articles about (N-Benzyl-norcodeinondimethylacetal-14-yl)-β-dimethylaminoethan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 145221-11-0
(N-Benzyl-norcodeinondimethylacetal-14-yl)acetamid

: 145221-14-3
(N-Benzyl-norcodeinondimethylacetal-14-yl)-β-dimethylaminoethan

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 3h; Heating;
DOI:10.1007/BF00812333

Reference yield:

: 100-39-0
benzyl bromide

: 145221-14-3
(N-Benzyl-norcodeinondimethylacetal-14-yl)-β-dimethylaminoethan

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / K₂CO₃ / acetone / 0.5 h / Heating

2: 83 percent / bromacetamide / CH₂Cl₂

3: 61 percent / 4 N NaOH, H₂ / Pd/C (10 percent Pd) / methanol / 3.5 h

4: 64 percent / xylene / 12 h / Heating

5: 1) 1 M LiAlH₄, 2) NaBH₄ / 1) THF, reflux, 2 h, 2) methanol

With sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; bromo-acetic acid amide; hydrogen; potassium carbonate; 10% palladium on active carbon; In methanol; dichloromethane; acetone; xylene;
DOI:10.1007/BF00812333

Reference yield:

: 145221-05-2
N-Benzyl-14-brom-norcodeinon-dimethylacetal

: 145221-14-3
(N-Benzyl-norcodeinondimethylacetal-14-yl)-β-dimethylaminoethan

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / 4 N NaOH, H₂ / Pd/C (10 percent Pd) / methanol / 3.5 h

2: 64 percent / xylene / 12 h / Heating

3: 1) 1 M LiAlH₄, 2) NaBH₄ / 1) THF, reflux, 2 h, 2) methanol

With sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen; 10% palladium on active carbon; In methanol; xylene;
DOI:10.1007/BF00812333