E,Z-1-<4-(N,N-bis-β-chloroethylcarbamoyloxy)-phenyl>-1,2-bis-(4-acetoxyphenyl)-but-1-ene

Base Information

Chemical Name:E,Z-1-<4-(N,N-bis-β-chloroethylcarbamoyloxy)-phenyl>-1,2-bis-(4-acetoxyphenyl)-but-1-ene
CAS No.:110008-63-4
Molecular Formula:C₃₁H₃₁Cl₂NO₆
Molecular Weight:584.496
Hs Code.:

Synonyms:E,Z-1-<4-(N,N-bis-β-chloroethylcarbamoyloxy)-phenyl>-1,2-bis-(4-acetoxyphenyl)-but-1-ene

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Chemical Property of E,Z-1-<4-(N,N-bis-β-chloroethylcarbamoyloxy)-phenyl>-1,2-bis-(4-acetoxyphenyl)-but-1-ene

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Technology Process of E,Z-1-<4-(N,N-bis-β-chloroethylcarbamoyloxy)-phenyl>-1,2-bis-(4-acetoxyphenyl)-but-1-ene

There total 5 articles about E,Z-1-<4-(N,N-bis-β-chloroethylcarbamoyloxy)-phenyl>-1,2-bis-(4-acetoxyphenyl)-but-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 110008-61-2
E,Z-1-<4-(N,N-bis-β-chloroethylcarbamoyloxy)-phenyl>-1,2-bis-(4-hydroxyphenyl)-but-1-ene

: 75-36-5
acetyl chloride

: 110008-63-4
E,Z-1-<4-(N,N-bis-β-chloroethylcarbamoyloxy)-phenyl>-1,2-bis-(4-acetoxyphenyl)-but-1-ene

Guidance literature:: With pyridine; at 60 ℃; for 1h;
DOI:10.1002/ardp.19903230407

Reference yield:

: 4390-94-7
1,2-bis(4-methoxyphenyl)butanone

: 110008-63-4
E,Z-1-<4-(N,N-bis-β-chloroethylcarbamoyloxy)-phenyl>-1,2-bis-(4-acetoxyphenyl)-but-1-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 2) aq. HCl / 1) ether, THF, 2h, reflux, 2) MeOH, 12h, room temp.

2: 42 percent / pyridine / 96 h / Ambient temperature

3: 35 percent / BBr₃ / CH₂Cl₂ / 2 h / -60 °C

4: 88 percent / pyridine / 1 h / 60 °C

With pyridine; hydrogenchloride; boron tribromide; In dichloromethane;
DOI:10.1002/ardp.19903230407

Reference yield:

: 36637-44-2
(4-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)magnesium bromide

: 110008-63-4
E,Z-1-<4-(N,N-bis-β-chloroethylcarbamoyloxy)-phenyl>-1,2-bis-(4-acetoxyphenyl)-but-1-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 2) aq. HCl / 1) ether, THF, 2h, reflux, 2) MeOH, 12h, room temp.

2: 42 percent / pyridine / 96 h / Ambient temperature

3: 35 percent / BBr₃ / CH₂Cl₂ / 2 h / -60 °C

4: 88 percent / pyridine / 1 h / 60 °C

With pyridine; hydrogenchloride; boron tribromide; In dichloromethane;
DOI:10.1002/ardp.19903230407