C₅₆H₇₂N₈O₁₇S₂

Base Information

Chemical Name:C₅₆H₇₂N₈O₁₇S₂
CAS No.:713122-19-1
Molecular Formula:C₅₆H₇₂N₈O₁₇S₂
Molecular Weight:1193.36
Hs Code.:

C<sub>56</sub>H<sub>72</sub>N<sub>8</sub>O<sub>17</sub>S<sub>2</sub>

Synonyms:C₅₆H₇₂N₈O₁₇S₂

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Chemical Property of C₅₆H₇₂N₈O₁₇S₂

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Technology Process of C₅₆H₇₂N₈O₁₇S₂

There total 20 articles about C₅₆H₇₂N₈O₁₇S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 713122-18-0
(Z)-D-Ser{Fmoc-D-Ser[Boc-L-Ala-L-Cys(Acm)-L-Val]-L-Ala-L-Cys(Acm)-L-Val}-OH

: 713122-19-1
C₅₆H₇₂N₈O₁₇S₂

Guidance literature:: With iodine; In methanol; dichloromethane; at 25 ℃; for 2.5h;
DOI:10.1021/jo0496805

Reference yield:

: 65806-90-8
(R)-2-(((benzyloxy)carbonyl)amino)-3-(tert-butoxy)propanoic acid

: 713122-19-1
C₅₆H₇₂N₈O₁₇S₂

Guidance literature:: Multi-step reaction with 11 steps

1: 78 percent / pyridine; HOBt; DCC / 18 h / 0 °C

2: 76 percent / TFA / 0.75 h / 10 °C

3: 88 percent / pyridine; HOBt; DCC / 18 h / 0 °C

4: TFA / 0.5 h / 25 °C

5: 3.80 g / HOAt; EDCI / CH₂Cl₂ / 18 h / 0 °C

6: TFA / 0.5 h / 25 °C

7: 3.18 g / HOAt; EDCI / CH₂Cl₂ / 16 h / 0 °C

8: TFA / 0.5 h / 25 °C

9: 52 percent / HOAt; EDCI / CH₂Cl₂ / 18 h / 0 °C

10: 94 percent / aq. AcOH; Zn powder / 2.5 h / 0 °C

11: 66 percent / I₂ / CH₂Cl₂; methanol / 2.5 h / 25 °C

With pyridine; 1-hydroxy-7-aza-benzotriazole; iodine; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; trifluoroacetic acid; zinc; In methanol; dichloromethane;
DOI:10.1021/jo0496805

Reference yield:

: 71989-33-8,128107-47-1
Nα-(9-fluorenylmethoxycarbonyl)-D-serine-tert-butyl ether

: 713122-19-1
C₅₆H₇₂N₈O₁₇S₂

Guidance literature:: Multi-step reaction with 11 steps

1: 66 percent / pyridine; HOBt; DCC / 18 h / 0 °C

2: 72 percent / TFA / 0.75 h / 10 °C

3: 73 percent / pyridine; HOBt; DCC / 18 h / 0 °C

4: TFA / 0.5 h / 25 °C

5: 2.06 g / HOAt; EDCI / CH₂Cl₂ / 18 h / 0 °C

6: TFA / 0.5 h / 25 °C

7: 1.41 g / HOAt; EDCI / CH₂Cl₂ / 16 h / 0 °C

8: 91 percent / aq. AcOH; Zn powder / 2.5 h / 0 °C

9: 52 percent / HOAt; EDCI / CH₂Cl₂ / 18 h / 0 °C

10: 94 percent / aq. AcOH; Zn powder / 2.5 h / 0 °C

11: 66 percent / I₂ / CH₂Cl₂; methanol / 2.5 h / 25 °C

With pyridine; 1-hydroxy-7-aza-benzotriazole; iodine; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; trifluoroacetic acid; zinc; In methanol; dichloromethane;
DOI:10.1021/jo0496805