5-Heptyl-3-methylsulfanyl-1,4-diphenyl-4H-[1,2,4]triazol-1-ium; iodide

Base Information

• Chemical Name: 5-Heptyl-3-methylsulfanyl-1,4-diphenyl-4H-[1,2,4]triazol-1-ium; iodide
• CAS No.: 77331-33-0
• Molecular Formula: C₂₂H₂₈N₃S*I
• Molecular Weight: 493.455
• Mol file: 77331-33-0.mol

Synonyms:5-Heptyl-3-methylsulfanyl-1,4-diphenyl-4H-[1,2,4]triazol-1-ium; iodide

Chemical Property of 5-Heptyl-3-methylsulfanyl-1,4-diphenyl-4H-[1,2,4]triazol-1-ium; iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Heptyl-3-methylsulfanyl-1,4-diphenyl-4H-[1,2,4]triazol-1-ium; iodide

There total 2 articles about 5-Heptyl-3-methylsulfanyl-1,4-diphenyl-4H-[1,2,4]triazol-1-ium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methyl-1,4-diphenyl isothiosemicarbazide (54211-56-2) → 5-Heptyl-3-methylsulfanyl-1,4-diphenyl-4H-[1,2,4]triazol-1-ium; iodide (77331-33-0)

Guidance literature:

DOI:10.1016/S0040-4039(00)93683-9

Reference yield:

heptanal (111-71-7) + 3-methylthio-1,4-diphenyl-1,2,4-triazolium chloride (77331-28-3) → 5-Heptyl-3-methylsulfanyl-1,4-diphenyl-4H-[1,2,4]triazol-1-ium; iodide (77331-33-0)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1016/S0040-4039(00)93683-9

Reference yield: 70.0%

5-Heptyl-3-methylsulfanyl-1,4-diphenyl-4H-[1,2,4]triazol-1-ium; iodide (77331-33-0) → methylthiol (74-93-1) + Octanoic acid (124-07-2) + 1,4-diphenylsemicarbazide (621-12-5)

Guidance literature:

With potassium hydroxide;

DOI:10.1016/S0040-4039(00)93683-9

upstream raw materials:

heptanal

3-methylthio-1,4-diphenyl-1,2,4-triazolium chloride

3-methyl-1,4-diphenyl isothiosemicarbazide

Downstream raw materials:

Octanal

methylthiol

Octanoic acid

1,4-diphenylsemicarbazide